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Extended Linear Chain Compounds Volume 1

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Beschreibung

Produktdetails

Einband

Gebundene Ausgabe

Erscheinungsdatum

31.03.1982

Abbildungen

XVI, 481 p.

Herausgeber

Joel S. Miller

Verlag

Springer Us

Seitenzahl

481

Gewicht

860 g

Auflage

1981

Sprache

Englisch

ISBN

978-0-306-40711-6

Beschreibung

Produktdetails

Einband

Gebundene Ausgabe

Erscheinungsdatum

31.03.1982

Abbildungen

XVI, 481 p.

Herausgeber

Joel S. Miller

Verlag

Springer Us

Seitenzahl

481

Gewicht

860 g

Auflage

1981

Sprache

Englisch

ISBN

978-0-306-40711-6

Herstelleradresse

Springer US, New York, N.Y.
Heidelberger Platz 3
14197 Berlin
Deutschland
Email: sdc-bookservice@springer.com
Fax: +49 6221 3454229

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  • Produktbild: Extended Linear Chain Compounds
  • Produktbild: Extended Linear Chain Compounds
  • 1. The Solution Properties of One-Dimensional Metal Chain Complexes.- 1. Introduction.- 2. Association of Square d8 Metal Complexes.- 2.1. Rhodium(I) Isocyanide Complexes; Self-Association.- 2.2. Iridium(I) Isocyanide Complexes; Self-Association.- 2.3. Chugaev’s Red Salt, (CH3NC)2Pt(C4H9N4)+X?; Self-Association.- 2.4. Pt(CN)24; Self-Association.- 2.5. [(RNC)4Pt][Pt(CN)4]; Ion Pairs.- 3. Mixed Valence Chain Compounds.- 3.1. Halide-Bridged Chains.- 3.2. Metal-Metal-Bonded Chains.- 3.3. Some Comments on the Mechanism of Formation of Mixed Valence Chain Compounds.- Notation.- References.- 2. Mass Spectrometry of Low-Dimensional Materials.- 1. Introduction.- 2. Instrumentation.- 2.1. Sample Introduction.- 2.2. Types of Ionization.- 2.3. Ion Separation.- 3. Mass Spectrometry Combinations.- 3.1. Pyrolysis Mass Spectrometry.- 3.2. Thermal Analysis Mass Spectrometry.- 3.3. Stress Mass Spectrometry.- 4. Mass Spectrometric Applications of Low-Dimensional Materials.- 4.1. Poly(sulfurnitride), polythiazyl, (SN)X.- 4.2. Polyacetylene.- 4.3. Graphite.- 5. Conclusion.- References.- 3. The Synthesis, Structure, Electrical Conduction Properties, and Theory of Divalent, Tetravalent, and One-Dimensional Partially Oxidized Tetracyanoplatinate Complexes.- 1. Introduction.- 2. Divalent Tetracyanoplatinates.- 2.1. Structural Studies.- 2.2. Optical Studies.- 2.3. Electrical Conduction Studies.- 3. Tetravalent Tetracyanoplatinates.- 3.1. Structural Studies.- 3.2. Solution, Optical, and Electrical Conduction Studies.- 4. Partially Oxidized Tetracyanoplatinate (POTCP) Metals.- 4.1. The Synthesis of POTCP Metals.- 4.2. The Molecular Structure of POTCP Metals.- 4.3. Anion-Deficient POTCP Salts.- 4.4. Cation-Deficient POTCP Salts.- 4.5. X-Ray Diffuse Scattering at Room Temperature and the Degree of Partial Oxidation.- 4.6. The Temperature Dependence of X-Ray Diffuse Scattering and Elastic Neutron Scattering.- 4.7. Inelastic Neutron Scattering, Infrared and Raman Spectroscopy.- 5. Summary and Discussion.- Notation.- References.- 4. Linear Chain Bis(oxalato)platinate Salts.- 1. Introduction.- 2. Survey of Reported Bis(oxalato)platinate Salts.- 3. Solution Chemistry of Bis(oxalato)platinate Salts.- 4. Degree of Partial Oxidation and the Peierls Superstructure.- 5. Structural Studies.- 5.1. Bis(oxalato)platinate(II) Salts.- 5.2. Partially Oxidized Bis(oxalato)platinate Salts.- 5.3. Non-Peierls Superstructures in Partially Oxidized Bis(oxalato)-platinate Salts.- 5.4. Intermodular Backbonding between Oxalate Ligands.- 6. Solid State Properties.- 6.1. Integral Oxidation State Salts.- 6.2. Partially Oxidized Salts.- 7. Comparison of the Properties of Partially Oxidized Bis(oxalato)platinate and Tetracyanoplatinate Salts.- 7.1. Type of Compound.- 7.2. Properties in Solution.- 7.3. Structural Features.- 7.4. Non-Peierls Superstructures.- 8. Conclusions.- Notation.- References.- 5. A Comprehensive Review of Linear Chain Iridium Complexes.- 1. Introduction.- 2. Halotricarbonyliridium Complexes: Ir(CO)3X, X=Cl, Br, or I.- 2.1. Syntheses and Physical Properties.- 2.2. X-Ray Structural Results.- 2.3. Analytical Results.- 2.4. Band Calculations.- 2.5. Mass Spectra.- 2.6. X-Ray Diffuse Scattering.- 2.7. Polarized Reflectance Spectra.- 2.8. Summary.- 3. Dihalodicarbonyliridate Complexes.- 3.1. Synthesis and Reactivity.- 3.2. Characterization and Physical Properties.- 3.3. Summary.- Notation.- References.- 6. Highly Conductive Halogenated Low-Dimensional Materials.- 1. Introduction.- 1.1. Strategies for Synthesizing Highly Conductive Low-Dimensional Materials.- 1.2. General Properties of Halogens Relevant to the Synthesis of Conducting Materials.- 2. Techniques for the Characterization of Halogens in Conductive Materials.- 2.1. Resonance Raman and Infrared Spectroscopy.- 2.2. Mössbauer Spectroscopy.- 2.3. Diffraction Techniques.- 2.4. Extended X-Ray Absorption Fine Structure (EXAFS).- 2.5. Optical Spectroscopy.- 2.6. Nuclear Quadrupole Resonance Spectroscopy.- 2.7. X-Ray Photoelectron Spectroscopy.- 3. General Synthetic Methodology.- 4. Stacked Organic Systems.- 4.1. Polycyclic Aromatic Hydrocarbons.- 4.2. Organonitrogen Systems.- 4.3. Organochalcogenide Systems.- 5. Stacked Metal-Organic Systems.- 5.1. Glyoximates and Related Materials.- 5.2. ?-Electron Tetraazaannulenes 271.- 5.3. ?-Electron Metallomacrocycles 278.- 5.4. Other Tetraazaannulenes.- 5.5. Thiolato Complexes.- 6. Stacked Inorganic Systems.- 7. Polymers.- 7.1. Organochalcogenide Systems.- 7.2. Poly(sulfurnitride), (SN)x.- 7.3. Polyacetylene.- 7.4. Face-to-Face Polymetallomacrocycles.- 8. Graphite.- 9. Conclusions and Prospects.- References.- 7. Structural Aspects of Iodine-Containing Low-Dimensional Materials.- 1. Introduction.- 2. Survey of Structures, Iodine Species, and Lattice Repeats.- 3. Relation between Stoichiometry and Structure: Prediction of Unknown Structures.- 4. Disorder in the Iodine Lattice.- 4.1. Types of Disorder in Columnar Structures and Their Manifestation in the X-Ray Pattern.- 4.2. Degrees of Disorder in N(CH3)3H(TCNQ)I.- 5. Iodine-Channel Wall Interactions.- 6. Comments on the Relative Stability of Various Iodine Species.- 7. Concluding Remarks.- Notation.- References.- 8. Linear Chain Platinum Haloamines.- 1. Introduction.- 2. Platinum(II) Compounds.- 2.1. Tetraammine- and Tetraammineplatinum(II) Chains [Pt(NH3)4]2+ and [PtL4]2+ Ions.- 2.2. Triamminehaloplatinum(II) Salts, [PtL3X]+Y?.- 2.3. Diamminedihaloplatinum(II), PtL2X2, Compounds.- 2.4. Aminetrihaloplatinates(II), [PtX3L]?Ions.- 2.5. Tetrahaloplatinates(II), [PtX4]2? Ions.- 3. Pt(II)-Pt(IV) Haloamine Mixed-Valence Materials.- 3.1. Chains of Dications [PtL4]2+[PtL4X2]2+ (Wolffram’s Salt Analogs).- 3.2. Chains of Monocations.- 3.3. Neutral Chains.- 3.4. Chains of Anions.- 3.5. Chains of Dianions.- 3.6. Comparison of Pt-X Pt Distances along the Different Chains.- 4. Conclusions.- Notation.- References.- 9. Optical Properties of Linear Chain Haloamine Platinum Complexes.- 1. Introduction.- 1.1. Types of Linear Chain Haloamine Complexes.- 1.2. Optical Spectra of Molecular and Ionic Species.- 2. Magnus-Type Compounds.- 2.1. Variations in Metal-Metal Spacings.- 2.2. Crystal Spectra of Magnus-Type Salts.- 3. Molecular Crystals.- 3.1. (Ethylenediamine)dichloroplatinum(II), Pt(en)Cl2.- 3.2. (Ethylenediamine)dibromoplatinum(II), Pt(en)Br2.- 3.3. Cis- and Trans-diamminedichloroplatinum(II).- 3.4. (Ethylenediamine)dichloropalladium(II), Pd(en)Cl2.- 4. Mixed-Valence Crystals.- 4.1. Molecular Crystals.- 4.2. Ionic Mixed-Valence Compounds.- 4.3. Octahedral PtIV Defect Inclusions in PtII Compounds.- 4.4. Nature of the Mixed-Valence Transition.- 4.5. Partially Oxidized Magnus’ Salt.- 5. Summary.- 5.1. Comparison of Haloamine Platinum and Palladium Systems.- 5.2. Contrasts between the Haloamine Platinum Systems and the One-Dimensional Conductors.- Notation.- References.